By Christoph A. Schalley
An summary of the options used to ascertain supramolecular aggregates from a methodological standpoint. Edited by means of a emerging megastar locally and an skilled writer, this can be a definitive survey of helpful sleek analytical equipment for figuring out supramolecular chemistry, from NMR to single-molecule spectroscopy, from electron microscopy to extraction tools. A definitive research of this box touching many interdisciplinary components equivalent to molecular units, biology, bioorganic chemistry, fabric technological know-how, and nanotechnology.
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Additional info for Analytical Methods in Supramolecular Chemistry
A. Deij, D. N. Reinhoudt, Angew. Chem. 2002, 114, 4647; Angew. Chem. Int. Ed. 2002, 41, 4467; b) A. Mulder, T. Auletta, A. Sartori, A. Casnati, R. Ungaro, J. Huskens, D. N. Reinhoudt, J. Am. Chem. Soc. 2004, 126, 6627; c) T. Auletta, M. R. de Jong, A. Mulder, F. C. J. M. van Veggel, J. Huskens, D. N. Reinhoudt, S. Zou, S. Zapotoczny, H. Scho¨nherr, G. J. Vancso, L. Kuipers, J. Am. Chem. Soc. 2004, 126, 1577. J. D. Badjic, V. Balzani, A. Credi, S. Silvi, J. F. Stoddart, Science 2004, 303, 1845. Reviews: a) J.
In addition, the required level of mathematical knowledge is not high, only a formula for polynomials of degree 2, therefore the logical basis can be easily understood. Moreover, statistical treatment of the obtained data is understandable with primary statistics. These are the merits to use this method at ﬁrst in order to understand the way of determination of binding constants. When stoichiometry of the complex is not 1 to 1 or when other premises are not satisﬁed, the way of data treatment should be changed or modiﬁed.
The origin of this error will be discussed and methods for avoiding these problems will be presented in the following three sections. Correlation between [H]0 , [G]0 , x and K The experimental conditions that can be set up by the experimenter are [H]0 and [G]0 (see Eq. 8) and classiﬁcation of variables). How should the experimental conditions, [H]0 and [G]0 , be changed for the titration? There are so many possibilities described graphically in Fig. 6 containing a dilution experiment, a continuous variation experiment, a constant [H]0 with diﬀerent [G]0 experiment and two more complicated examples.